PhD Thesis In: cienciavitae

CARACTERIZAÇÃO DA RESISTÊNCIA À FRACTURA E FADIGA DE MATERIAIS CERÂMICOS ESTRUTURAIS

Jorge Cruz Fernandes1994

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Authors:

Supervisors:

Luís Guerra Rosa

Published in

November 1994

Abstract

The aim of this work was to investigate the influence of different testing methodologies on the values of strength and toughness of ceramic materials (at room temperature and high temperatures). Three materials were selected for this research: tungsten carbide (with 4wt% cobalt content), high purity alumina and alumina containing 7wt% zirconia. These materials were extensively characterized in terms of microstructure. Young moduli were determined through bending and ressonance tests. Four point bending strength was determined and compared to values obtained by equibiaxial bending. The influence of surface roughness on the flexural strength was assessed. Weibull statistics was used to analyse the data. Tests carried out using unnotched specimens allowed to investigate some particular aspects such as the influence of jig articulation and of the static fatigue parameter n. Results of four point bending and KIc at high temperature (800oC; 1000oC e 1200oC) are also presented for alumina and alumina/zirconia. Four methods, Indentation Fracture, Indentation Strength by Bending, Single Edge Notch Beam and Double Torsion were applied to evaluate the fracture toughness (including in equibiaxial loading). The advantages and/or experimental problems encountered in each of those methods are discussed and guidelines for the correct use of these methods are presented.

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Fields of Science and Technology (FOS)

materials-engineering - Materials engineering

Publication language (ISO code)

por - Portuguese

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